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Compact 1100℃ Tube Furnace for CVD Growth of 2D Layers of TMDs
Compact 1100℃ Tube Furnace for CVD Growth of 2D Layers of TMDs

Compact 1100℃ Tube Furnace for CVD Growth of 2D Layers of TMDs

Model:KJ-1200X-UL

Description:

KJ-1200X-4-NW-UL is a compact 1100°C CVD tube furnace with precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition.

Detailed

Specific Introduction:
    KJ-1200X-4-NW-UL is a compact 1100°C CVD tube furnace with precursor sublimating attachment. Totally four-channel gas inlets are built on the sublimation which allows feedings of various gases to carry the source vapor into the main heater for further decomposition and deposition. The sample holder fixture mounted on the right flange is slidable for easy sample loading/unloading. Such a system configuration is suitable for growing a wide range of transitional metal dichalcogenides (such as MoSe2, MoS2...) and wide bandgap semiconductors (such as h-BN) layers on substrate up to 3" diameter. 

Parameters:

Furnace and Preheater Compact CVD furnace system is modified from kj-1200X-100 single zone tube furnace:
  • 4.33" O.D x 4.05" I.D x 29.13" Length quartz tube
  • 1100ºC Max. working temperature
  • The water cooling flange on the right-side is slidable for easy sample loading
  • Water cooling flange on the left-side between the heater and furnace is used for pre-heated gas input and sealing
Four-channel gas inlet ( 1/8" Dia tube and tube fitting) are built-in on the left side flange
 
One small heater is attached to the left side flange of the furnace to preheat input gas, liquid,  or evaporate solid chemical, which will be then delivered to the CVD furnace:
1.2''O.D x 6''L SS tube as the heating chamber
600ºC Max. working temperature
The flange on the left side is for gas sealing and input
Rated Voltage Single Phase, 220V AC, 50/60 Hz, AWG 8# Power cord is included (without plug)
Power consumption Max. 3600 W (20 A breaker required)

Heating Zone
  • CVD Furnace:  440 mm
  • Constant temperature zone: 100 mm 
  • Gas Heater:     150mm



Working Temperature
  • CVD Furnace:
    • Max heating temperature: 1100°C ( < 2 hour )
    • Continuous working temperature: 200~1000°C
    • Max heating & cooling rate: 20°C/min
  • Heater:
    • Continuous working temperature: RT~600°C
    • Max heating & cooling rate: 20°C/min
Temperature Control
 
  • CVD Furnace and Heater (separate temp control):
Digital controllers with PID/self-tuning functions and 30 segments programmable
Thermocouple:  K type thermocouples, which feed through the right side flange and control furnace temperature.
Control accuracy: +/- 1°C
RS485 Communications Port













Vacuum
and Gas Sealing & Flange
 
The right flange of the CVD furnace
  • Water cooling to prevent sealing o-ring from melting (water cooler is not included)
  • KF25 vacuum fitting (to a vacuum pump, please contact us to order a pump,  vacuum hose, valve and sealing gasket)
  • Slidable for the customer to easily and fast push/pull in/out a sample
  • One quartz wafer holder ( 3" Dia. ) is included and the flange with heating radiation block 
  • An anti-corrosive capacitance diaphragm gauge is included
Left flange (between CVD Furnace and Heater) with four 1/8'' Swagelok fittings for 1/8'' tube:
  • Two 1/8'' fitting on the flange for independently and directly delivering any gas into the CVD furnace 
  • One 1/8'' fitting for delivering heated gas from heater to CVD furnace
  • One 1/4'' fitting for bypassing the gas (without heating) to the CVD furnace (inside the CVD furnace, the gas tube is merged with the heated gas pipe by a T fitting)
Note: How gas pipe assembled in the CVD furnace through above 1/8'' fitting:
  • One 1/4'' quartz tube delivers the vapor gas from the heater(also the bypass gas by a T fitting)
  • Two 1/4'' quartz tube delivery extra gas via the two separate 1/8'' fitting on the big furnace left the flange
  • These three 1/4'' quartz tubes inside the CVD furnace is in parallel and vertically 1'' higher than the sample holder
  •  These three 1/4'' quartz tubes can be easily removed to clean or replaced once get stuck or corroded
Heater:
  • Left flange: one 1/8'' gas fitting to deliver gas to the heater for pre-heating and then to the CVD furnace On the right side to the CVD furnace with necessary thermal block material to minimize the temperature gradient at the interface between the heater and CVD furnace
  • Furnace Chamber Installation
  • 2- 1/4" pipe adapter is installed on each flange
The optional Liquid Injection device (optional) For direct liquid CVD  ( DLCVD), you may consider devices for liquid injection
Net weight 110kg
Dimensions
 
  • Standard:    62"L X 18"W X 23"H
  • Maximum:   80"L X 18"W X 32"H  (Lid open and right-side flange slided out)
Warranty One year limited warranty for electrical parts. ( Consumable parts such as processing tubes, o-rings and etc are not covered by the warranty)
Compliance
    
  • CE Certified
  • NRTL(UL61010)  or CSA certifications are available at extra cost. 
Warning
 
  • The tube furnaces with quartz tube are designed for use under vacuum and low pressure <0.2 bars (relative to 1 atm, absolute pressure = 1.2 bar if used in air)
  • Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. 
  •  Vacuum pressures may only be safely used up to 1000°C 
  • The flow rate for gasses should be limited to< 200ml/min) for reducing thermal shocks to the tube

Compact 1100℃ Tube Furnace

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